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在水溶剂中,采用水热法合成了含氮配体化合物[H(2phen)2C6H5S2O6N]·2H2O(phen=1,10-邻菲罗啉).采用X射线单晶衍射和元素分析等方法对其进行了表征.X射线单晶衍射表征结果表明,该配合物晶体属于三斜晶系.研究了该化合物的紫外可见光谱以及热稳定性.该化合物紫外可见光谱的峰在315nm,热稳定性良好.“,”In aqueous solvent, the compound of [H(2phen)2C6H5S2O6N]·2H2O(phen=1,10-phenanthroline)containing N-donor ligand was syn-thesized by hydrothermal method.The X-ray single crystal diffraction and elemental analysis were used to characterize the compound. And the results showed that the compound belonged to the triclinic system. The UV-Vis spectrum and thermal stability of the compound were also investigated. The peak of the UV-vis spectrum of the compound was at 315 nm.And it had a good thermal stability.