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以钨丝为工作电极研究了氟化物熔盐体系中镁的电化学沉积,分别用原子发射光谱与X射线荧光光谱法对阴极产物进行了判定,结果表明,在本研究条件下,阴极产物为金属镁,循环伏安法和计时电位法的测定结果表明,电极过程受含镁离子在熔体中的扩散控制。
The tungsten electrode was used as the working electrode to study the electrochemical deposition of magnesium in fluoride molten salt system. The products of cathode were determined by atomic emission spectrometry and X-ray fluorescence spectroscopy respectively. The results showed that under the conditions of this study, the cathode product was The determination results of metal magnesium, cyclic voltammetry and chronopotentiometry show that the electrode process is controlled by the diffusion of magnesium ions in the melt.