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本文作者之一在前一篇所发表的工作中,曾据根切林齐夫测定活泼氢方法的原理,设计了一套同时测定活泼氢及“CH_3MgI 试剂加成”的仪器;同时描述了测定的方法,并给出了几个测定的结果.这个新的方法可以代替所谓“Kohler 机器”,而且具备仪器装置比较简单、操作手续也较简便等优点.为了进一步改善这个方法的仪器装置和简化操作方法,并对较广泛地应用这个方法作些探讨,本文作者又进行了这一工作.
In the work published in the previous article, one of the authors of this paper devised a set of instruments for the simultaneous determination of active hydrogen and “CH 3 MgI reagent addition” based on the principle of gen- , And gives the results of several measurements.This new method can replace the so-called “Kohler machine”, but also has the advantages of simple instrumentation, simple procedures, etc. In order to further improve the instrumentation and simplification of this method Methods of operation, and to explore this more widely used methods, the author of this article has carried out this work.