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在乙醇胺及甘油和乙二胺混合物两种非水介质中合成了全硅方钠石,在广泛的有机介质中进行了全硅沸石合成的研究,首次获得了全硅ZSM-39及未知结构硅酸盐K相,通过X射线衍射、红外光谱、组成分析、差热与热重分析等方法对合成的晶体产物进行了鉴定,应用液相电导率-硅酸根离子浓度测量方法对非水溶液的性质及对非水介质中全硅沸石生成的必要条件进行了探讨。
In the ethanolic amine and glycerol and ethylenediamine mixture of two non-aqueous media synthesis of all sodalite in a wide range of organic media for the study of all-zeolite synthesis, for the first time obtained all-silicon ZSM-39 and unknown structure of silicon The K phase was characterized by X-ray diffraction, infrared spectroscopy, compositional analysis, differential thermal analysis and thermogravimetric analysis. The results of liquid phase conductivity-silicate ion concentration measurement on the properties of non-aqueous solution And the necessary conditions for the formation of all-zeolite in non-aqueous media were discussed.