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提出了采用示波极谱法测定馏分油及石油产品中元素硫的方法。支持电解液是含有０．５ｍ ｏｌ／Ｌ醋酸和０．３ ｍ ｏｌ／Ｌ醋酸铵体积比为１∶１的甲苯－甲醇溶液。在此介质中，饱和甘汞电极的峰电位为－ ０．６１Ｖ。该方法灵敏度高，当元素硫浓度为０．１ ｍ ｇ／Ｌ时仍可以看到明显峰电流；精密度和准确度较好，对１ ｍ ｇ／Ｌ元素硫的测定，标准偏差为０．０２；元素硫浓度在０～４ ｍ ｇ／Ｌ浓度范围与极谱峰电流呈线性关系。
A method for the determination of elemental sulfur in distillate oil and petroleum products by oscillopolarography was proposed. The supporting electrolyte is a toluene-methanol solution containing 0.5 mol / L acetic acid and 0.3 mol / L ammonium acetate in a 1: 1 volume ratio. In this medium, the peak potential of the saturated calomel electrode is -0.61V. The method has high sensitivity and obvious peak current can still be seen when elemental sulfur concentration is 0.1 m g / L. The precision and accuracy are good. The standard deviation of elemental sulfur of 1 m g / L is zero. 02; elemental sulfur concentration in the range of 0 ~ 4 m g / L concentration and polarographic peak current was linear.